Compendium of Organic Synthetic Methods -Volume 11 by Michael B. Smith

By Michael B. Smith

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Souma, Y. J. Org. , 2000, 65, 1540. ; Souma, Y. J. Org. , 2000, 65,8105. A 1. (R0)2BH, Rh(d);BF4-, 0 p 2 H * 2. LiCIIC12 3. ; -- BINAP Ph . n Ph * 9 9 ~ 8 7 %(93% ee, R) c::: J. Org. , 1999, 64, 9704. ; Johnstone. W, Chem. , 1999, 37. 16 Compendium of Organic Synthetic Methods, Vol 11 4 PdClZ(PPh3h, COM20 * /I,,H TsOI1, LiCl Ph Org. , 1999, I , 459. ; Section 30 91 % REVIEWS: "Palladium-Catalysed Reppe Carbonylation," SECTION 30: Chem. , 2001, 101,3435. ; Sakurai, H. , 2001, 42, 1961. PhCH=N-OI 1 * PhC02H 99% 30% HzOz, THF , reflux, 10 h Synth.

SECTION 27: ACID DERIVATIVES FROM KETONES aq Oxone, NaHC03 w ~ Ph r L . Lee. C. J. Org. , 2001, 66, 1523. C. Synlett, 2001, 1563. , 1999, 40, 6077. Zabjek, A,; sA. A RQO,, 70% TBIIP, 5 h Ph Gurunath, S . ; Sudal ai. A. Synlctt, 1999, 559. PhCOOH 71% Section 29 Acids from Alkenes 0 1. ; Mlochowski, J. Synth. , 1999, 29, 2281. 5 h Bu Bu Kahalka. ; Tmtman, S. Synth. , 1999, 29, 2783. 67% SECTION 28: ACID DERIVATIVES FROM NITRILES - NO ADDITIONAL EXAMPLES SECTION 29: ACID DERIVATIVES FROM ALKENES 1 atm C O , H 2 0 , H2S04 [Rh(C0)41+ ,fi * 3('02H68% Xu.

Dai. : Hao. J, Tctruhedron Asymin. 2001, 12, 2613. ; Gau. , 2001, 12, 2971. A. J. Chem. , Perkin Trans. 1, 2001, 854. ; PhCAO -1 Ph Et 99% (87% ee) Chem. , 2000, 2471. , 2000, 41, 4587. -S. , 2000, 11, 4923. g\/SnBu3 PhCHO , aq EtOH , 4 O " C * (9-tolyl-BINAP , AgN03, 14 h 93% (79% ee) Loh. -R. , 2000, 41, 5261. , 2000, 41, 8813. = CHO 1. allyldialkoxytitanium complex ether, -78°C 2. ; Falguibres, A. , 2000, 41, 8877. 1) PhMezSi QIi - -- BOW), MeCHO 2) I I 2 0 2 , pH 6 huffer 3) Na$03, 0" * 80% (93%ee) SiMqPh h u s h .

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